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Unopex B 230 Pilot Scale Spray Dryer has been designed for small scale productions, for scientific test works in the universities and R&D departments and for scale up studies. Unopex B 230 Pilot Scale Spray Dryer is suitable for production of powders from solutions, suspensions or emulsions. The powder characteristics can be controlled and powder properties maintained constant throughout a continuous operation.

We offer a great range of hemp-derived raw materials. These are various ingredients that can be used for the production of cosmetics, foodstuffs and food supplements, vape oils for e-cigarettes and other consumer products. Here we have gathered all essential characteristics of raw materials with varying potencies in terms of cannabinoids such as CBD, cannabinol (CBN), cannabigerol (CBG). Samples of all products are also available – you can buy a sample for your own analysis, for the development or for the pilot-scale production of your product.

Product Identification Chemical name: 2-Chlorodimethylsilylindene Synonyms: Chloro(1H-inden-2-yl)dimethylsilane, Chloro-(1H-inden-2-yl)dimethylsilane, Chloro-2-Indenyldimethylsilane, Chloro-2-Indenyl-Dimethylsilane CAS No.: 240823-57-8 Molecular formula: C11H13ClSi Molecular weight: 208.76 Boiling point: 274 ℃ @ 760 mmHg Density: 1.050 g/mL Specification Appearance: Colorless to pale yellow transparent liquid Purity: 90.00%min by GC Package Regular Packing: N.W 5kg/plastic drum Sample Packing: 0.1kg-0.5kg glass bottle Transportation Information Classification: Non-dangerous goods HS Code: 2903999090 Status & Application Status Pilot scale Application 2-Chlorodimethylsilylindene [240823-57-8] is used to produce [(2-indenyl)-(2-phenyl-1-indenyl)dimethylsilyl] zirconium dichloride, Me2Si(2-Ind)(2-Ph-1-Ind)ZrCl2. Me2Si(2-Ind)(2-Ph-1-Ind)ZrCl2 is a catalyst of polypropylene.

Product Identification Chemical name: 4'-Nitrobenzo-15-crown-5 Synonyms: 4-Nitrobenzo-15-crown-5, 4'-Nitrobenzo-15-crown-5 ether, 4-Nitrobenzo-15-crown-5 ether, 2,3-(4-Nitrobenzo)-1,4,7,10,13-pentaoxacyclopentadec-2-ene CAS No.: 60835-69-0 Molecular formula: C14H19NO7 Molecular weight: 313.30 Melting point: 93-97 ºC Specification Appearance: Pale yellow solid Purity: 98.00%min by HPLC Moisture: 0.50%max by KF Package Regular Packing: N.W 25kg/fiber drum Sample Packing: 0.1kg-1kg foil bag or under request Transportation Information Classification: Non dangerous goods HS Code: 2932999090 Application Chloroform–water extraction systems have been studied using crown-ethers as extracting agents, namely: benzo-15-crown-5 (B15C5), 2,3-naphtho-15-crown-5 (N15C5), 4′-nitro-benzo-15-crown-5 (NO2B15C5), 4′-tert-butyl-benzo-15-crown-5 (TBB15C5), and 4′-acetyl-benzo-15-crown-5 (AcB15C5).

Product Identification Chemical name: Tris(2-pyridylmethyl)amine Synonyms: Tris(pyridin-2-ylmethyl)amine, TPMA, Tripicolylamine CAS No.: 16858-01-8 Molecular formula: C18H18N4 Molecular weight: 290.36 Melting point: 85-89 ℃ Specification Appearance: White to off-white solid Purity: 98.00%min by HPLC Clarity: Clear in 10% acetonitrile solution Moisture: 0.50%max by KF Package Regular Packing: N.W 25kg/fiber drum Sample Packing: 0.1kg-1kg foil bag or under request Transportation Information Classification: Non-dangerous goods HS Code: 2921590090 Application Tris(2-pyridylmethyl)amine is a tripodal ligand, mainly used to simulate the coordination environment within some proteins. It is also used as a copper ligand in ATRP.

Product Identification Chemical name: 2,4,6-Triphenylpyrylium tetrafluoroborate Synonyms: 2,4,6-Triphenylpyrylium tetrafluoroborate, 2,4,6-Triphenylpyrylium fluoroborate, 2,4,6-Triphenyl-pyrylium tetrafluoroborate CAS No.: 448-61-3 Molecular formula: C23H17OBF4 Molecular weight: 396.19 Melting point: 252-254 ºC Specification Appearance: Yellow powder Purity: 98.00%min by HPLC Moisture: 0.50%max by KF Package Regular Packing: N.W 1kg/vacuum foil bag Sample Packing: 0.1kg-0.5kg vacuum foil bag or under request Transportation Information Classification: Non-dangerous goods HS Code: 2942000000 Status & Application Polit Scale 2,4,6-Triphenylpyrylium tetrafluoroborate is used as a sensitizer to carry out the photo oxidation of cathecol. It is also used in the preparation of photosensitizers.

Product Identification Chemical name: 3,5-Dihydroxybenzaldehyde Synonyms: α-Resorcylaldehyde CAS No.: 26153-38-8 Molecular formula: C7H6O3 Molecular weight: 138.12 Melting point: 159-160 ℃ Specification Appearance: White to gray crystalline powder Purity: 98.00%min by GC Package Regular Packing: N.W 10kg/fiber drum Sample Packing: 0.1kg-0.5kg foil bag Transportation Information Classification: Non-dangerous goods HS Code: 2912499090 Status & Application Status Commercial available Application: Used for organic synthesis

Product Identification Chemical name: Methoxytriethyleneoxypropyltrimethoxysilane Synonyms: Methoxytriethyleneoxypropyltrimethoxysilane, 3,3-dimethoxy-2,7,10,13,16-pentaoxa-3-silaheptadecane CAS No.: 132388-45-5 Molecular formula: C13H30O7Si Molecular weight: 326.46 Boiling point: 140.0 °C @ 0.2 mmHg Density: 1.163 g/mL Refractive index: 1.432 Specification Appearance: Colorless transparent liquid Purity: 97.00%min by GC Package Regular Packing: N.W 20kg/plastic drum Sample Packing: 0.1kg-1kg plastic bottle or under requests Transportation Information Classification: Non-dangerous goods HS Code: 2931900090 Status & Application Status Commercial available Application Methoxytriethyleneoxypropyltrimethoxysilane [132388-45-5] is used in the application: 1. Composition for forming coating film; 2. Touch panel and solar cell;

Product Identification Chemical name: 2,3-Diamino-6-chlorobenzonitrile Synonyms: 3-Cyano-4-chloro-1,2-benzenediamine CAS No.: 548457-80-3 Molecular formula: C7H6ClN3 Molecular weight: 167.60 Specification Appearance: White to off-white solid Purity: 99.00%min by HPLC Moisture: 0.50%max Package Regular Packing: N.W 25kg/fiber drum Sample Packing: 0.1kg-0.5kg/plastic bottle Transportation Information Classification: Non dangerous goods HS Code: 2921590090 Status & Application Status Pilot scale Application: Pharmaceutical intermediate

Product Identification Chemical name: 3-Methoxy-4,5-dihydroxyphenethylamine Synonyms: 5-(2-Aminoethyl)-3-methoxybenzene-1,2-diol CAS No.: 16032-86-3 Molecular formula: C9H13NO3 Molecular weight: 183.21 Melting point: 190-192 ℃ Specification Appearance: Brown solid Purity: 95.00%min by HPLC Mositure: 0.5%max Package Regular Packing: N.W 5kg/plastic drum Sample Packing: 0.1kg-0.5kg plastic bottle Transport Information Classification: Non-dangerous goods HS Code: 2921499090 Status & Application Status: Commercial available Application: Pharmaceutical intermediate

Product Identification Chemical name: 2-Acetoxystyrene Synonyms: 2-Vinylphenyl acetate, Acetic acid 2-vinylphenyl ester CAS No.: 63600-35-1 Molecular formula: C10H10O2 Molecular weight: 162.19 Boiling point: 246 ℃ @ 760 mmHg Density: 1.070 g/mL Refractive index: 1.547 Specification Appearance: Colorless transparent liquid Purity: 98.00%min by GC Clarity (10% methanol solution): Clear Moisture: 0.10%max by KF Residual solvents: 0.10%max Polymerization inhibitor: 200-300 ppm Package Regular Packing: N.W 20kg/plastic drum Sample Packing: 0.1kg-1kg plastic bottle Transportation Information Classification: Non-dangerous goods HS Code: 2915390090 Status Commercial available Application 2-Acetoxystyrene [63600-35-1] has application in monomers for the production of resins, elastomers, adhesives, coatings, automotive finishes and inks, as well as in electronic materials. It may also be used as additives in elastomer and resin formulations.

Product Identification Chemical name: 5-(Trifluoromethyl)dibenzothiophenium tetrafluoroborate Synonyms: S-(Trifluoromethyl)dibenzothiophenium tetrafluoroborate CAS No.: 131880-16-5 Molecular formula: C13H8BF7S Molecular weight: 340.07 Melting point: 162-164 ºC Specification Appearance: Yellow solid Purity: 98.00%min by GC Moisture: 0.50%max by KF Package Regular Packing: N.W 10kg/fiber drum Sample Packing: 0.1kg-1kg plastic bottle or under request Transportation Information Classification: Non-dangerous goods HS Code: 2920900090 Status Pilot scale Application 5-(Trifluoromethyl)dibenzothiophenium tetrafluoroborate [131880-16-5] is a type of useful, shelf-stable electrophilic umemoto reagent, mainly used as a trifluoromethylating reagent.

Product Identification Chemical name: 5-(Trifluoromethyl)dibenzothiophenium tetrafluoroborate Synonyms: S-(Trifluoromethyl)dibenzothiophenium tetrafluoroborate CAS No.: 131880-16-5 Molecular formula: C13H8BF7S Molecular weight: 340.07 Melting point: 162-164 ºC Specification Appearance: Yellow solid Purity: 98.00%min by GC Moisture: 0.50%max by KF Package Regular Packing: N.W 10kg/fiber drum Sample Packing: 0.1kg-1kg plastic bottle or under request Transportation Information Classification: Non-dangerous goods HS Code: 2920900090 Status Pilot scale Application 6-Hydroxy-1-tetralone[3470-50-6] is mainly used as pharmaceutical intermediate.

Product Identification Chemical name: 4-Phenylbenzamidine hydrochloride Synonyms: [1,1'-Biphenyl]-4-carboximidamide hydrochloride, 4-phenylbenzenecarboximidamide hydrochloride, [1,1'-Biphenyl]-4-carboximidamide monohydrochloride, Biphenyl-4-carboxamidine hydrochloride CAS No.: 111082-23-6 Molecular formula: C13H13ClN2 Molecular weight: 232.71 Melting point: 247-252 ºC Specification Appearance: White to off white powder Purity: 98.00%min by HPLC LOD: 0.50%max by K-F Package Regular Packing: N.W 20kg/fiber drum Sample Packing: 0.1kg-1kg plastic bottle or under request Transportation Information Classification: Non-dangerous goods HS Code: 2925290090 Status & Application Status: Pilot scale Application: Used for preparing 1, 3, 5 - triazine derivatives, which are a series of very important OLED intermediates

Product Identification Chemical name: 4-Bromo-2,6-di-tert-butylanisole CAS No.: 1516-96-7 Synonyms: 5-Bromo-1,3-di-tert-butyl-2-methoxybenzene, 3,5-di-tert-butyl-4-methoxybromobenzene, 1-bromo-3,5-di-tert-butyl-4-methoxybenzene, 1-Bromo-4-methoxy-3,5-di-tert-butylbenzene Molecular formula: C15H23BrO Molecular weight: 299.25 Melting point: 49-50 ºC Specification Appearance: Beige powder Purity: 98.00%min by GC Package Regular Packing: N.W 25kg/fiber drum Sample Packing: 0.1kg-1kg foil bag or under request Transportation Information Classification: Non-dangerous goods HS Code: 2909309013 Status & Application Status: Pilot scale

Product Identification Chemical name: 10-Undecen-1-ol Synonyms: 10-Undecenol, Undec-10-enol, Undec-10-en-1-ol, 10-Hendecen-1-ol CAS No.: 112-43-6 Molecular formula: C11H22O Molecular weight: 170.29 Boiling point: 245.0-245.5 ºC Density: 0.850g/mL @ 25°C Flash point: 125 ºC Refractive index: 1.4460-1.4509 Specification Appearance: Colorless transparent liquid Purity: 97.00%min by GC Package Regular Packing: N.W 20kg/plastic drum Sample Packing: 0.1kg-1kg plastic bottle or under request Transportation Information Classification: Non-dangerous goods HS Code: 2905290000 Status & Application Status: Pilot scale Application: Used as a flavoring & perfume agent. Used as a material of 10-Undecen-1-ol Homopolymer It reacts with tosylated beta-cyclodextrin to prepare beta-cyclodextrin undecenylether. It is used in the synthesis of 10-Undecenylacrylat by reacting with acryloyl and triethylamine.

Product Identification Chemical name: 11-Bromo-1-undecene Synonyms: 1-Bromo-10-undecene, 10-Undecenyl bromide CAS No.: 7766-50-9 Molecular formula: C11H21Br Molecular weight: 233.19 Boiling point: 251.6 ºC Density: 1.067g/mL @ 25°C Flash point: 110.3 ºC Refractive index: 1.4505-1.4700 Specification Appearance: Colorless transparent liquid Purity: 97.00%min by GC Package Regular Packing: N.W 20kg/plastic drum Sample Packing: 0.1kg-1kg plastic bottle or under request Transportation Information Classification: Non-dangerous goods HS Code: 2903399090 Status Pilot scale Application Mainly used for organic synthsis. It reacts with triethylsilane to prepare (11-bromoundecyl)triethoxysilane. It is used in capping porous dielectrics. Reference: MERCK PATENT GMBH; BOBADE, Sachin; POLISHCHUK, Orest; PADMANABAN, Munirathna; BASKARAN, Durairaj WO2019/81450, 2019, A1

For dependable and reproducible hydrogenations Buchi gas dosing system bpc 2 in combination with Buchi pressure reactors creates an optimal solution for safe, accurate and reproducible hydrogenations. The Buchi hydrogenator is a turnkey hydrogenation solution, consisting of: bpc 2 (Buchi pressflow controller) for hydrogen dosing, control of reaction pressure and continuous measuring of the Hydrogen uptake until saturation Buchi pressure reactors, offered in different materials and volumes for high to low pressure applications The unique volumetric hydrogen gas dosing records the parameters pressure, momentary consumption and overall consumption. The optional bls3 allows Operation of the apparatus via PC and storing or recorded data for further analyses.

Glass pilot reactor and pilot plant Glass reactor: 15, 30, 60 liter Pressure: -1.0 (FV) to +0.5 bar Temperature: -60 °C (-90 °C) to +200 °C Material: Borosilicate glass 3.3, glass-lined steel, PTFE, PFA, tantalum A clean-room setup and other materials are available to meet your specific process requirements. Performance and reliability are key issues in the explosion proof design of Buchi glass reaction systems. The inert materials allow safe processing in an inert atmosphere of a wide range of solvents and acids in a completely sealed glass reaction system under full vacuum. Multiple chemical reaction steps are performed safely in the same setup. The system consists of: Reactor, solid jacketed full view glass reactor to easily improve and control chemical reactions by visual observation Distillation glass overhead built with buchiflex components (unique flexible ball - socket joints) for mulitple, reliable processes under full vacuum

Pressure reactor for kilo labs and small-scale production Reactor volume: 20 to 500 liter Pressure: -1 (FV) to +200 bar Temperature: -20 °C to +300 °C Material: stainless steel, Hastelloy® Other materials, pressures & temperatures are available Buchi pilot plants are built for pressure reactions as well as for reactions under full vacuum. Different technologies and materials are used, depending on the requested process and process media. Pilotclave pressure reactors range from 50 - 500 liter and are all customized. To quote such systems we require detailed specifications. Safety is important with such larger scale systems, especially when doing hydrogenations and other reactions under higher pressure. The degree of automation and process control vary from simple data collection to complete automation of the system. In most cases, the reaction vessels are jacketed steel or Hastelloy® reactors.

Basic glass reactor systems for API synthesis, small scale production and pilot plant. Glass reactor: 15, 30, 60 liter Pressure: -1.0 (FV) to +0.5 bar Temperature: -60 °C (-90 °C) to +200 °C Material: Borosilicate glass 3.3, glass-lined steel, PTFE, PFA, Tantalum A clean-room setup and other materials are available to meet your specific process requirements. Performance and reliability are key issues in the explosion proof design of Buchi glass reaction systems. The inert materials allow safe processing in an inert atmosphere of a wide range of solvents and acids in a completely sealed glass reaction system under full vacuum. Multiple chemical reaction steps are performed safely in the same setup. The system consists of: Solid jacketed full view glass reactor to easily improve and control reactions by visual observation Distillation glass overhead built with buchiflex components (unique flexible ball - socket joints) for multiple, reliable processes under full vacuum

High-performance reactor systems for API synthesis, small scale production and pilot plant applications Glass, glass-lined steel reactor: 15, 30, 60, 100, 160, 250 liter Pressure: -1.0 (FV) to +0.5 bar Temperature: -60 °C (-90 °C) to +200 °C Material: Borosilicate glass 3.3, glass-lined steel, PTFE, PFA, tantalum A clean-room setup and other materials are available to meet your specific process requirements. Performance and reliability are key issues in the explosion proof design of Buchi glass reaction systems: The inert materials allow safe processing in a inert atmosphere of a wide range of solvents and acids in a completely sealed glass reaction system under full vacuum. Multiple chemical reaction steps are performed safely in the same setup. The system consists of:

The Rotavac One is our complete compact pilot filter station. Easy to install and operate it is ideal for small volume applications, process validation and pilot-scale trials. The unit has a small 2m x 1m footprint, comprising of 1.3m² skid mounted rotary vacuum drum filter (RDVF), filtrate receiver, filtrate pump, vacuum pump, blower (scraper discharge version only), local control panel. Two versions are available: Rotavac One S, scraper discharge and Rotavac One P, precoat discharge. These filters are ideal for larger test programmes under actual manufacturing conditions. We can provide filter media from our extensive range and advise on this if required. Please contact us for more information if you are interested in purchase or hire of our pilot filter.

Filtration Services offer a range of filtration equipment for hire. We have Rotavac Lab (lab scale) and Rotavac One (pilot scale) rotary drum vacuum filters and tipping pan filters available for immediate hire. Please contact us If you have any questions, or require information on any of our filters that are available for hire.

The Rotavac Lab is a fully functional and representative lab scale rotary drum vacuum filter (RDVF) and filtration system, generally used for product evaluation tests or as a preliminary step towards pilot scale and full scale equipment trials. The unit can be used to validate the suitability of this type of continuous vacuum filtration equipment. The equipment offers the advantage of an easily interchangeable discharge system so that different configurations can be trialled if required. It is supplied with a control panel for modifying drum and agitator speeds and, when using a precoat discharge, the knife advance rate. A separate skid mounted feed tank, mixer and feed pump is included with the RDVF. The unit is easy to assemble and we can provide full detailed instructions including photographs at the point of hire. We include filter cloths from our extensive range of fabrics. Please contact us for more information if you are interested in purchase or hire of this lab filter.

BS-pilotDRY® Series ML001 - ML010 The pilotdryer BS-pilotDRY from BOLZ is well suited for a wide range of various pilot-scaled trials and tests within the product and process development, but also for ongoing quality monitoring of a production. Mainly used as a traditional conical screw dryer, in addition it can also be used as a central shaft dryer. The hybrid stirrer technology allows drying and mixing processes to be simulated and tested in only one appliance using different mixing tools. Therefore relevant comparisons are possible which facilitate the selection of the most suitable stirring mechanism or agitator tool for the product and thus for the future production equipment. Special properties for the customer’s benefit: Mobile and portable skid design Simple „plug and use“ installation Complete process unit with ancillaries Flexible filling volume 10 to 100% CIP-cleaning included All product contact surfaces heatable Suited for a wide range of processes Ideal for...

Memcell classic The MEMCELL plant has been developed to run laboratory trial with minimized effort. The plant is suitable for membrane screening, cleaning examinations, lab trials and quality management. All common flat sheet membranes can be used. The plant is suitable for the following processes: Ultrafiltration Nanofiltration Reverse osmosis The flat module corresponds in his hydraulic properties to a spiral wound element. So, examinations with the flat module can be used for up-scaling to pilot plant sizes. The flat cell is available with various spacers (30-44-80mil); to run the plant with another spacer, only the middle part of the test cell has to be changed. On permeate side, there is a porous sinter plate to guarantee a steady permeate flow. So, a reliable scale-up is possible. For membrane manufacturer or technical institutes, the MemCell is available on request with parallel or seriell connection of more than one test cell. Technical data: Working pressure 64 bar (standard)

Unequalled for design and capabilities, the Genesis is the most versatile freeze dryer for pilot, research or small scale production applications. Its advanced product monitoring and process control make it ideal for research and with a user-friendly interface it is perfect for laboratories with multiple products or formulations to investigate. An ergonomic layout allows easy inspection of the vacuum pump and facilitates oil changes, which can be made quickly and cleanly in the laboratory environment. Genesis is available with up to six bulk drying shelves (five vial processing shelves). An expanded range of shelf arrangements, available with a shelf latching kit, allows you to configure it to process a wide variety of vial sizes.

Hamon Research-Cottrell provides process and equipment expertise, drawn from more than fifteen years of experience with the patented Urea to Ammonia U2A® technology, starting from bench and pilot scale, through systems for small gas turbine SCR and the largest utility scale SCR systems for coal and gas fired boilers.Hamon Research-Cottrell’s U2A® system provides several benefits:Urea as feedstock eliminates the hazards associated with the transport, transfer and storage of toxic anhydrous or aqueous ammonia.Compared with using 19% aqueous ammonia, energy use is reduced.Process control response provides ammonia on demand, easily following load conditions.Hamon Research-Cottrell offers U2A® on a worldwide basis and has installations in Europe and the Middle East in addition to a large installed base in the United States.